ISO 6502 provides guidance on the determination of vulcanization characteristics of rubber compounds by means of curemeters.
DIN 53529 specifies a method of determining the vulcanization characteristics of rubber mixes with the aid of curemeters and of evaluating cross-linking isotherms in terms of reaction kinetics. A description of the apparatus required is given in DIN 53 529 Part 1 and DIN 53 529 Part 3 deals with the determination of cross-linking behavior with the aid of rotorless curemeters.
ASTM D 5289 is used to determine the vulcanization characteristics of (vulcanizable) rubber compounds. This test method may be used for quality control in rubber manufacturing processes, for research and development testing of raw-rubber compounded in an evaluation formulation, and for evaluating various raw materials used in preparing (vulcanizable) rubber compounds.
The test specimen in a rotorless cure meter approaches the test temperature in a shorter time and there is a better temperature distribution in the test specimen due to the elimination of the unheated rotor found in oscillating disk cure meters. Several manufacturers produce rotorless cure meters with design differences that may result in different torque responses and cure times for each design. Correlations of test results between cure meters of different designs should be established for each compound tested, and for each set of test conditions.
ASTM D 6204 is used to measure viscoelastic properties of raw rubber as well as unvulcanized rubber compounds. These viscoelastic properties may relate to factory processing behavior.
This test method may be used for quality control in rubber manufacturing processes and for research and development testing of raw rubber and rubber compounds. This test method may also be used for evaluating compound differences resulting from the use of different compounding materials.
This test method covers the use of a rotorless oscillating shear rheometer for the measurement of the flow properties of raw rubber and unvulcanized rubber compounds. These flow properties are related to factory processing.
ASTM D 6601 is used to determine the vulcanization characteristics of (vulcanizable) rubber compounds under selected test conditions of strain and frequency which do not significantly affect the cured dynamic properties. In the same test, this test method also will measure the dynamic properties of the vulcanizate at temperatures significantly below the cure temperature. These lower temperature measurements are necessary in order to more effectively relate to rubber product service conditions.
This test method may be used for quality control in rubber manufacturing processes and for research and development testing of rubber compounds containing curatives. This test method also may be used for evaluating cure and dynamic property differences resulting from the use of different compounding ingredients.
This test method covers the use of a rotorless oscillating shear rheometer for measuring after cure dynamic properties at predetermined temperature(s) below the cure temperature.